MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\BIZ\\BIZ2016-D07-WJ6.D Tgt Mass (EZX): 395.00 Injection Date : 7 Dec 16 3:51 pm +0800 Seq. Line : 0 Sample Name : BIZ2016-D07-WJ6 Location : P2-B-04 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-10562A Batch#22739 Easy-Access Method: '1-POS-3MIN' 395.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU20001500100050000.5*DAD1 C, Sig=254,4 Ref=off mAU60020001.20940011.2721.2721.2091.4551.522.5min*1.3091.6320.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701500001000005000001.2641.522.5min*0.511.5 Ion 396, MSD1 396,Target Mass 395 +H Positive, EIC=395.7:396.7 10000075000500002500000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.51.26422.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.02 3.22 0.44 0.16 317 1.27 0.01 1965.24 2520.37 99.76 396 1.45 0.01 1.48 2.01 0.08 317 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.02 1.29 0.53 0.19 317 1.27 0.01 661.13 920.83 98.44 396 1.31 0.03 7.95 4.27 1.18 396 1.63 0.02 1.21 0.85 0.18 317HY-LCMS-02 12/7/2016 16:09:02 KFF(LCMS-02)Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.26 <<<< POSITIVE SPECTRA >>>> ES-API Positive30000250002000015000 317.31000050000200300400500600700800900m/z 397.3 396.2HY-LCMS-02 12/7/2016 16:09:02 KFF(LCMS-02)Page 2 of 2