MS Report from Instrument: LCMS-03 File ..a\\20171017\\20171017-1\\BIZ2017-O17-WYQ15.D Tgt Mass (CHM): Injection Date : 17 Oct 17 4:55 pm +0800 Seq. Line : 5 Sample Name : BIZ2017-O17-WYQ15 Location : P2-B-07 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\\LCMS03\\Data\\20171017\\20171017-1\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20171017\\20171017-1\\1-POS-3MIN.M Catalog No: HY-107382 Batch#26700 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off500250000.5 DAD1 B, Sig=254,4 Ref=offmAU10000.5 ELS1 A, ELSD SignalmV400200000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7040000002000000000.51 Ion 482.3, MSD1 482.3,Target Mass 482.3 Positive, EIC=482:4831.522.5min1.4171.522.5min11.4501.522.5min11.3821.436mAU1.5901.522.5min2000000.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.38 0.02 883.17 750.84 98.24 483 1.44 0.02 14.37 13.28 1.60 483 1.59 0.01 1.44 1.75 0.16 483 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.42 0.07 25080152.00 6039553.00 100.00 483LCMS-03 10/18/2017 9:11:18 SYSTEMPage1 of3MS Report from Instrument: LCMS-03Ret. Time: 1.42 <<<< POSITIVE SPECTRA >>>> ES-API Positive483.11.2E61E68000006000004000002000000100200300400500600700800900m/z485.1484.1LCMS-03 10/18/2017 9:11:18 SYSTEMPage2 of3MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 10/18/2017 9:11:18 SYSTEMPage3 of3